HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → (E)-3-[4-(3-Dimethylaminopropenyl)phenyl]acrylic Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | (E)-3-[4-(3-dimethylaminopropenyl)phenyl]acrylic acid, methyl ester | HCID 86755260 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | (E)-3-[4-(3-Dimethylaminopropenyl)phenyl]acrylic Acid | HCID 70098974 | 85% |
Reaktionsschritte
This product was prepared by refluxing for four hours, (E)-3-[4-(3-dimethylaminopropenyl)phenyl]acrylic acid, methyl ester with NaOH (0.16 g, 2 equiv.) in 10 mL of MeOH. After evaporation of the solvent in vacuo, treatment with 5 mL of HCl (1N) gave the title compound (0.4 g, 85%) as a gummy orange solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06117881 |
| Quelldatensatz | uspto-grants-2000_09 |
| ORD ID | ord-4732a76e30ec461c99139977ab9ac3cd |
| Quellennotiz | uspto-grants-2000_09 |