HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86755261, compound → HCID 22252158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86755261 | HCID 86755261 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22252158 | HCID 22252158 | 40% |
Reaction Steps
The same method as employed in the preparation of Example 79 but starting a solution of (E)-(4-[3-oxo-3-(1-(3,4-methylenedioxyphenyl)-1,3,4,9-tetrahydro-βcarbolin-2-yl)propenyl]benzyloxy)acetic acid, ethyl ester in EtOH gave after recrystallization from MeOH:H2O the title compound as an off-white solid in a 40% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117881 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-6c95957ffc104cce9c329598b42d06f3 |
| Source note | uspto-grants-2000_09 |