Isobutyl 2-aminobutyrate → HCID 53904087, compound

HRID 1953586Notes

Reaction equation

HRID 1953586 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[C:9]([CH2:10][C:11]([OH:13])=O)[C:4]=2[N:3]=[CH:2]1.[NH2:14][CH:15]([CH2:23][CH3:24])[C:16]([O:18][CH2:19][CH:20]([CH3:22])[CH3:21])=[O:17]>>[CH2:19]([O:18][C:16](=[O:17])[CH:15]([NH:14][C:11](=[O:13])[CH2:10][C:9]1[C:4]2[N:3]=[CH:2][S:1][C:5]=2[CH:6]=[CH:7][CH:8]=1)[CH2:23][CH3:24])[CH:20]([CH3:21])[CH3:22]

Participants

3

Reactant 2

HCID 13743360Isobutyl 2-aminobutyrateHCID 23298462(1,3-Benzothiazol-4-yl)acetic acid

Product 1

HCID 53904087HCID 53904087, compound

Procedure

Following General Procedure I above and using 4-benzothiazol-yl acetic acid (Chemservice) and iso-butyl 2-aminobutyrate (prepared following General Procedure J above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.

Workup

  1. customThe reaction was monitored by tlc on silica gel and purification
  2. filtrationwas by filtration

Sources & evidence

ORD record
ord-d5e9ab9c4ec8413c9c0f4dddda1d4536
Source dataset
uspto-grants-2000_09
Patent number
US06117901

Reaction notes

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