Dodecylphosphate → HCID 86755834, compound

HRID 1953636Notes

Reaction equation

HRID 1953636 reaction equation
[P:1]([O-:27])([O-:26])([O:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])=[O:2].[P:28]([O-:44])([O-:43])([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH3:42])=[O:29]>>[P:1]([O-:26])([O-:27])([O:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])=[O:2].[P:28]([O-:43])([O-:44])([O:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH3:42])=[O:29]

Participants

3

Reactant 2

HCID 1550836DodecylphosphateHCID 21997214HCID 21997214, compound

Product 1

HCID 86755834HCID 86755834, compound

Conditions

Temperature
70 °C

Procedure

To a stirred vessel was added 60 percent w/w of the PEG-5 behenyl phosphate of Example 2 and 40 percent w/w of the lauryl phosphate of Example 1. The vessel contents were heated to 70° C. and allowed to mix for 30 minutes, and then recovered as a mixture of mono- and diester phosphates of PEG-5 behenyl alcohol and lauryl alcohol having an acid value of 169.5 mg KOH.

Workup

  1. additionto mix for 30 minutes
  2. customrecovered as a mixture of mono- and diester phosphates of PEG-5 behenyl alcohol and lauryl alcohol having an acid value of 169.5 mg KOH

Sources & evidence

ORD record
ord-bb7d272db9fc4c288725f2d2a70713dd
Source dataset
uspto-grants-2000_09
Patent number
US06117915

Reaction notes

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