HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 2-Amino-5-chloro-3-nitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 2-Amino-5-chloropyridine | HCID 66174 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 2-Amino-5-chloro-3-nitropyridine | HCID 224168 | — |
Reaction Steps
A procedure similar to that described in Preparation 56 was repeated, except that 25.0 g of 2-amino-5-chloro-pyridine, 100 ml of concentrated sulfuric acid and 12.5 ml of concentrated nitric acid were used, to give 18.5 g of the title compound, melting at 138-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117893 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-ac29baa7d1a2494db1d935b11292ea59 |
| Source note | uspto-grants-2000_09 |