HCID 178483604, compound → CID 64738

HRID 1953928Notes

Reaction equation

HRID 1953928 reaction equation
[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:11]([O-:20])(=[O:19])[C:12]1[C:13](=[CH:15][CH:16]=[CH:17][CH:18]=1)[OH:14].[C:21]([O-:30])(=[O:29])[C:22]1[C:23](=[CH:25][CH:26]=[CH:27][CH:28]=1)[OH:24].[Mg+2:31].[OH:32][CH2:33][CH2:34][N+:35]([CH3:38])([CH3:37])[CH3:36]>O>[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:11]([O-:20])(=[O:19])[C:12]1[C:13](=[CH:15][CH:16]=[CH:17][CH:18]=1)[OH:14].[C:21]([O-:30])(=[O:29])[C:22]1[C:23](=[CH:25][CH:26]=[CH:27][CH:28]=1)[OH:24].[Mg+2:31].[OH:32][CH2:33][CH2:34][N+:35]([CH3:38])([CH3:37])[CH3:36].[C:1]([O:10][CH2:17][CH2:18][N+:35]([CH3:37])([CH3:36])[CH3:34])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[Mg+2:31].[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4]

Participants

6

Reactant 1

HCID 178483604HCID 178483604, compound2×

Product 4

HCID 64738CID 64738HCID 130354332-(2-Hydroxybenzoyl)oxyethyl-trimethylazaniumHCID 178483604HCID 178483604, compoundHCID 178524311Salicylate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A 10% solution of anionic salicylate was prepared by dissolving 10 g of choline magnesium trisalicylate (Trilisate™, Purdue Frederick, Norwalk, Conn.) in 87 g of distilled water. The mixture was stirred until the choline magnesium trisalicylate was fully dissolved. Each gram of choline magnesium trisalicylate yielded 587 mg of choline salicylate, 725 mg of magnesium salicylate being equivalent to 1 gram of salicylate content. Final composition:

Workup

  1. dissolutionwas fully dissolved

Sources & evidence

ORD record
ord-7225513ac9304a5285794a41bdd68eda
Source dataset
uspto-grants-2000_09
Patent number
US06120756

Reaction notes

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