HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178505549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Reactant | 4-Fluorobenzamidine | HCID 4295238 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178505549 | HCID 178505549 | — |
Reaction Steps
To a two-phase mixture of 30% K2CO3 solution (5 ml) and chloroform (5 mL) containing 276 mg of 4-fluorobenzamidine was added a solution of 468 mg of 2-bromo-4'-chloroacetophenone in chloroform (3 mL). After stirring for 1 hr, the reaction mixture was filtered. The white crystallinesolid was washed with distilled water and dried in a vacuum oven overnight to afford 2-(4-fluorophenyl)4-(4-chlorophenyl)imidazole (Compound 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06121260 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-48bb087bcd0b4f4ea42f7eb7d7388d78 |
| Source note | uspto-grants-2000_09 |