HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzylamine → 3-Chloro-4-(2,4-dichlorobenzylaminocarbonyl)-6-(4-pyridyl)pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzylamine | HCID 1485 | — |
| Reactant | 3-Chloro-4-chlorocarbonyl-6-(4-pyridyl)pyridazine | HCID 15895227 | — |
| Product | 3-Chloro-4-(2,4-dichlorobenzylaminocarbonyl)-6-(4-pyridyl)pyridazine | HCID 12085105 | — |
Reaction Steps
The title compound was prepared by treating the dichloride (6) with 2,4-dichlorobenzylamine according to Scheme I. DCI-MS m/z 392 (m+H+). 1H NMR (CDCl3) δ 8.83 (d, J=6 Hz, 2H), 8.33 (a, 1H), 8.00 (d, J=6 Hz, 2H), 7.5 (m, 2H), 7.3 (m, 3H), 4.76 (d, J=6 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06121266 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-28300cb7c6184c0d8cc358af2b615db3 |
| Source note | uspto-grants-2000_09 |