Thionyl Chloride → HCID 23296067, compound

HRID 1954042Notes

Reaction equation

HRID 1954042 reaction equation
[CH2:1]([C:3]1([CH2:17][CH3:18])[CH2:7][C:6]2=[C:8]([C:14](O)=[O:15])[CH:9]=[CH:10][C:11]([O:12][CH3:13])=[C:5]2[O:4]1)[CH3:2].S(Cl)([Cl:21])=O>C1(C)C=CC=CC=1>[CH2:1]([C:3]1([CH2:17][CH3:18])[CH2:7][C:6]2=[C:8]([C:14]([Cl:21])=[O:15])[CH:9]=[CH:10][C:11]([O:12][CH3:13])=[C:5]2[O:4]1)[CH3:2]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 22438534HCID 22438534, compound

Product 1

HCID 23296067HCID 23296067, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Analogously to Example A1, 1.2 g of 2,2-diethyl-2,3-dihydro-7-methoxybenzofuran-4-carboxylic acid are reacted in a mixture of 10 ml of toluene and 2 ml of thionyl chloride.

Sources & evidence

ORD record
ord-b3dfe03230e24297966490f2e120417b
Source dataset
uspto-grants-2000_09
Patent number
US06121274

Reaction notes

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