HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethoxyphenethylamine → N-(2, 3-dimethoxyphenylethyl)-2-(3,4-dimethoxyphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethoxyphenethylamine | HCID 137858 | — |
| Reactant | (3,4-Dimethoxyphenyl)acetyl chloride | HCID 3604458 | — |
| Product | N-(2, 3-dimethoxyphenylethyl)-2-(3,4-dimethoxyphenyl)acetamide | HCID 22742672 | — |
Reaction Steps
prepared from 2,3-dimethoxyphenethylamine (Lindemann, Helv. Chim. Acta. 1949, 32, 69-75) and 3,4-dimethoxyphenylacetyl chloride; mp 80° C. (lit.29 79-80° C.); IR 3315, 2962, 2838, 1636, 1593, 1548; 1H NMR δ 2.61 (t, 2H), 3.22-3.30 (m, 4H), 3.58 (s, 3H), 3.64 (s, 6H), 3.67 (s, 3H), 6.22 (brs, 1H), 6.44-6.79 (m, 6H); 13C NMR δ 30.0, 41.0, 43.7, 55.9, 56.2, 56.3, 60.9, 111.2, 111.9, 112.9, 122.0, 122.6, 124.4, 127.9, 133.1, 147.5, 148.5, 149.5, 153.1, 171.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06121275 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-55296d6af4d14de4a1e74d49635d8ace |
| Source note | uspto-grants-2000_09 |