HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 9871467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-(3-chloropropyl)piperidine hydrochloride | HCID 79624 | — |
| Reactant | 2-(4-Methoxyphenyl)-3-(3-hydroxyphenyl)-6-methoxybenzo[b]thiophene | HCID 15485303 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9871467 | HCID 9871467 | 66.8% |
Reaction Steps
A manner similar to that used in Example 1, 3.09 g (8 mmol) of 2-(4-Methoxyphenyl)-3-(3-hydroxyphenyl)-6-methoxybenzo[b]thiophene, 2.4 g (12 mmol) of 1-(3-chloropropyl)piperidine hydrochloride, 5.5 g (40 mmol) of K2CO3 in 200 mL of DMF was coverted to 2.8 g of the title compound, isolated as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06121293 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-2540cdeb0a824f6f9c6843a1c8c5883d |
| Source note | uspto-grants-2000_09 |