Tin tetrachloride → HCID 21193478, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure in Example 1, step 4 using 3-cyclopentyl-4-methoxy-benzoic acid (10.00 g, 45.4 mmol, RN-59216-82-9), oxalyl chloride (4.4 mL, 50.4 mmol), N,N-DMF (5 drops), tin(IV) chloride (5.8 mL, 49.7 mmol) and 2-benzyl-4,5-dimethylfuran (10.1 g, 54.3 mmol) in CH2Cl2. The final organic extracts were concentrated to give 18.8 g of the title compound, synthetically pure. 1H NMR: consistent.

Provenance & Evidence