Thiophenol → 4-Sulfanylbenzaldehyde

HRID 1954332Notes

Reaction equation

HRID 1954332 reaction equation
[SH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[CH:9]([O:11]C)Cl>>[SH:1][C:2]1[CH:7]=[CH:6][C:5]([CH:9]=[O:11])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7969ThiophenolHCID 21004Methane, dichloromethoxy-

Product 1

HCID 109205784-Sulfanylbenzaldehyde

Procedure

The above reaction of Example 21A is repeated except that the starting materials are mercaptobenzene and dichloromethyl methylether. Using the same reaction conditions and techniques, there is obtained 4-mercaptobenzaldehyde.

Workup

  1. customThe above reaction of Example 21A
  2. customthe same reaction conditions and techniques

Sources & evidence

ORD record
ord-e2e9250e970b4b0c9ad0436530bc7f79
Source dataset
uspto-grants-2000_09
Patent number
US06121321

Reaction notes

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