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HRID1954340

反应详情

EQUATION

反应方程式

HRID 1954340 的结构方程式

REACTANTS

反应物

2
结构：O=C(CCl)N1CCCC1
HCID88440

1-(Chloroacetyl)pyrrolidine

C6H10ClNO

结构：CCOC(=O)c1c2ccc(CC(=O)NO)ccc-2c(C(=O)OCC)c1N.[Na]
HCID86755843

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1c2ccc(CC(=O)NOCC(=O)N3CCCC3)ccc-2c(C(=O)OCC)c1N
HCID15411820

未命名化合物

收率 24%

PROCEDURE

实验过程

In an analogous manner to that described in Example 1, from diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium and N-chloroacetyl-pyrrolidine the title compound of m.p. 168-170° C. is obtained in 24% yield.