HRID1954350

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID66918

3-Chloropropyl(diethyl)amine

C7H16ClN

结构：CCOC(=O)c1c2ccc(CC(=O)NO)ccc-2c(C(=O)OCC)c1N.[Na]

HCID86755843

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)c1c2ccc(CC(=O)NOCCCN(CC)CC)ccc-2c(C(=O)OCC)c1N

HCID23296742

未命名化合物

收率 42%

PROCEDURE

实验过程

In an analogous manner to that described in Example 1, from diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium and 3-diethylamino-propyl chloride the title compound of m.p. 125-127° C. is obtained in 42% yield.