Sodium Hydroxide → HCID 23296553, compound

HRID 1954360Notes

Reaction equation

C([O:3][C:4]([CH2:6][N:7]1[C:11]2[CH:12]=[CH:13][C:14]([N:16]([S:22]([CH3:25])(=[O:24])=[O:23])[CH2:17][CH2:18][N:19]([CH3:21])[CH3:20])=[CH:15][C:10]=2[N:9]=[C:8]1[CH2:26][O:27][C:28]1[CH:33]=[CH:32][C:31]([C:34](=[NH:36])[NH2:35])=[CH:30][CH:29]=1)=[O:5])C.[OH-].[Na+]>>[OH:5][C:4]([CH2:6][N:7]1[C:11]2[CH:12]=[CH:13][C:14]([N:16]([S:22]([CH3:25])(=[O:23])=[O:24])[CH2:17][CH2:18][N:19]([CH3:21])[CH3:20])=[CH:15][C:10]=2[N:9]=[C:8]1[CH2:26][O:27][C:28]1[CH:33]=[CH:32][C:31]([C:34](=[NH:35])[NH2:36])=[CH:30][CH:29]=1)=[O:3]

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 23296528HCID 23296528, compound

Product 1

HCID 23296553HCID 23296553, compound

Procedure

Prepared analogously to Example 3 from 1-ethoxycarbonylmethyl-2-[(4-amidinophenyl)-oxymethyl]-5-[N-(2-dimethylaminoethyl)-methanesulphonylamino]-benzimidazole and sodium hydroxide solution.

Sources & evidence

ORD record: ord-f69b47b7070c482581bf80b978970a84
Source dataset: uspto-grants-2000_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06121308

Reaction notes

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