HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-Quinolinesulfonyl chloride → HCID 23296439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-Quinolinesulfonyl chloride | HCID 29220 | — |
| Reactant | HCID 23296465 | HCID 23296465 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 23296439 | HCID 23296439 | — |
Reaction Steps
A mixture of 2.3 g (7.74 mmol) of 2-[(4-cyanophenyl)methylthio]-6-amino-benzothiazole and 1.85 g (8.1 mmol) of quinoline-8-sulphonic acid chloride is stirred in 30 ml of pyridine for 2 hours at ambient temperature. Then the solvent is distilled off in vacuo and the crude product is purified by flash chromatography (silica gel, methylene chloride/ethanol=99:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06121308 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-2941bd7214414a56a55cc0684c6cd7c3 |
| Source note | uspto-grants-2000_09 |