Potassium Hydroxide → HCID 86755848, compound

HRID 1954469Notes

Reaction equation

HRID 1954469 reaction equation
[OH-].[K+:2].[C:3]([CH2:5][CH2:6][N:7]([C:12](=[O:24])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[CH2:8][C:9]([OH:11])=[O:10])#[N:4]>>[C:3]([CH2:5][CH2:6][N:7]([C:12](=[O:24])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[CH2:8][C:9]([O-:11])=[O:10])#[N:4].[K+:2]

Participants

3

Reactant 2

HCID 14797Potassium HydroxideHCID 10935820HCID 10935820, compound

Product 1

HCID 86755848HCID 86755848, compound

Procedure

A 30% aqueous solution of KOH was gradually added to the N-cyanoethyl-N-dodecanoylglycine obtained in Example 2 to thereby adjust the pH of the system to 6.0. Thus, an aqueous solution of potassium N-cyanoethyl-N-dodecanoylglycinate was obtained. 1H-NMR spectrum (200 MHz, D2O) 4.02 (s,1 H), 3.94 (s,1 H), 3.76 (t,1 H), 3.65 (t,1 H), 2.80 (t,1 H), 2.71 (t,1 H), 2.50 (t,1 H), 2.30 (t,1 H), 1.60 (m,2 H), 1.31 (b,16 H), 0.89 (t,3 H) ppm

Sources & evidence

ORD record
ord-26f8a25c7cb6440787517c022ee6fb38
Source dataset
uspto-grants-2000_09
Patent number
US06121470

Reaction notes

Loading…