2-Propanethiol → HCID 23293463, compound
Reaction equation
S([C:5]1[N:6]=[C:7]2[N:11]([C:12]=1C(OCC)=O)[CH:10]=[CH:9][S:8]2)(C)(=O)=O.[CH:18]([SH:21])([CH3:20])[CH3:19]>>[CH:18]([S:21][C:5]1[N:6]=[C:7]2[N:11]([CH:12]=1)[CH:10]=[CH:9][S:8]2)([CH3:20])[CH3:19]Participants
3
Procedure
In a manner similar to the procedure in Reference Example 1, the oily title compound was prepared from ethyl 6-mesylimidazo[2,1-b]thiazole-5-carboxlate and isopropyl mercaptan. ##STR10## NMR(CDCl3) δ: 1.30(s, 6H), 3.15-3.65(m, 1H), 6.85(d, 1H), 7.38(d, 1H), 7.62(s, 1H)
Sources & evidence
- ORD record
- ord-47731b65ad3a4d159240b99a28771194
- Source dataset
- uspto-grants-2000_09
- Patent number
- US06124243
Reaction notes
Loading…