Dichloromethane → HCID 23293649, compound

HRID 1954905Notes

Reaction equation

HRID 1954905 reaction equation
[F:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]([CH3:15])[CH2:7]/[C:8]/2=[CH:11]\[C:12](O)=[O:13])=[CH:4][CH:3]=1.[Cl:16]CCl>>[F:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]([CH3:15])[CH2:7]/[C:8]/2=[CH:11]\[C:12]([Cl:16])=[O:13])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6344DichloromethaneHCID 23293638HCID 23293638, compound

Product 1

HCID 23293649HCID 23293649, compound

Procedure

This compound was prepared in an analogous manner to Example 15h with the replacement of (E)-2-(6-fluoro-3,3-dimethyl-1-indanylidene)acetic acid with (E)-2-(6-fluoro-3-methyl-1-indanylidene)acetic acid (9 g, 43.6 mmol). The product residue was dissolved in dichloromethane and used, without purification, in Example 17, 18, and 19.

Workup

  1. customused, without purification, in Example 17, 18, and 19

Sources & evidence

ORD record
ord-fb1f4e82004a431a8362eb58d1310045
Source dataset
uspto-grants-2000_09
Patent number
US06124284

Reaction notes

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