HCID 23294875, compound → HCID 15895988, compound

Participants

Reaction Steps

To a solution of 1-[3,5-dimethoxy-4-(methoxymethoxy)-phenyl]-2-nitro-1-ethanol (11.78 g, 41.0 mmol) in ethanol (100 ml) was added 10% palladium on charcoal (3.5 g), followed by hydrogenation at room temperature for 6 hours. After completion of the reaction, the catalyst was filtered off. The filtrate was concentrated, whereby the title compound (8.57 g, yield: 81.6%) was obtained as colorless crystals.

Provenance & Evidence