HuagongsheHuagongshe Chemistry Print Report · For research reference only
Gamma-Butyrolactone → HCID 67513941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Gamma-Butyrolactone | HCID 7302 | — |
| Reactant | Oleylamine | HCID 5356789 | — |
| Product | HCID 67513941 | HCID 67513941 | — |
Reaction Steps
Oleylamine (125 g, tech grade, 80% pure, 0.374 mole) was heated with γ-butyrolactone (27 ml, 0.35 mole) at 180° C. under nitrogen for 24 hours. The product was purified via vacuum distillation as a light yellow waxy solid. Mass Spectra: m/e (relative intensity) 335 (M+, 28.40).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124365 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-462f6fa27b174fa09dc592dccf0c75f8 |
| Source note | uspto-grants-2000_09 |