HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthol → 2-((1-Naphthalenyloxy)methyl)oxirane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthol | HCID 7005 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | 2-((1-Naphthalenyloxy)methyl)oxirane | HCID 91521 | — |
Reaction Steps
A mixture of 1-naphthyl alcohol, chloromethyloxirane, potassium carbonate and methylethylketone was heated at reflux for 5 hours to give 2-(1-naphthyloxy)methyloxirane. This intermediate was treated with 4-benzylpiperidine to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124323 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-f771f3a637f144948efb0b41d8f8891a |
| Source note | uspto-grants-2000_09 |