HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanopyridine → HCID 23294327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanopyridine | HCID 7506 | — |
| Reactant | 2-Bromonaphthalene | HCID 11372 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 23294327 | HCID 23294327 | — |
Reaction Steps
4-((2-Naphthyl)methyl)pyridine was prepared from 2-bromonaphthalene, n-BuLi and 4-cyanopyridine in two steps as a yellow solid: mp 66-67° C., 1H NMR (CDCl3) 4.13 (s, 2H), 7.14 (d, J=6.0 Hz, 2H), 7.27 (dd, J=5.7 and 1.8 Hz, 1H), 7.42-7.52 (m, 2H), 7.64 (s, 1H), 7.74-7.86 (m, 3H), 8.51 (dd, 4.8 and 1.5 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124323 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-b4825e64720b4cd389edc9d02b6a6e99 |
| Source note | uspto-grants-2000_09 |