HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1955435Generated: October 31, 2026
Thionyl Chloride → Benzylthiocarbonyl chloride
https://huagongshe.com/reaction/1955435
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178526157 | HCID 178526157 | — |
| Product | Benzylthiocarbonyl chloride | HCID 19906501 | 92% |
Reaction Steps
A quantity of 762 g (4.536 mol) of 2-phenylthioacetic acid is stirred at room temperature for 3 hours with thionyl chloride (375 ml, 5.14 mol), then stirred at 40° C. for 3 hours. Rotary evaporation followed by bulb-to-bulb distillation gives 777 g (4.166 mol, 92%) of 2-phenylthioacetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06124475 |
|---|
| Source dataset | uspto-grants-2000_09 |
|---|
| ORD ID | ord-74ca1e928adc4ad3b81bd498d193a74a |
|---|
| Source note | uspto-grants-2000_09 |
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