1,2-Benzenedicarbonitrile, 3-nitro- → HCID 19070339, compound

Participants

Reaction Steps

As in Synthesis Example 1 but using 1.73 grams of 1,2-dicyano-3-nitrobenzene and 3.40 grams of 2-t-butyl-6-methylcyclohexanol, there was obtained 1.48 grams of 1,2-dicyano-3-(2-t-butyl-6-methylcyclohexyloxy)benzene (yield of 50%). Next, as in Synthesis Example 1 but using 1.48 grams of this benzene compound and 0.42 gram of BBr3, there was obtained 1.1 grams of the end product (yield 68%, mp 154°-155° C.).

Provenance & Evidence