2-Tert-Butylphenol → HCID 19070334, compound

Participants

Reaction Steps

As in Synthesis Example 1 but using 1.73 grams of 1,2-dicyano-4-nitrobenzene and 3.0 grams of 2-t-butyl-hydroxybenzene, there was obtained 2.2 grams of 1,2-dicyano-4-(2-t-butylphenyloxy)benzene (yield of 80%). Next, as in Synthesis Example 1 but using 1.38 grams of this benzene compound and 0.42 gram of BBr3, there was obtained 0.77 gram of the end product (yield 50%, mp 163°-165° C.).

Provenance & Evidence