HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl carbamate → 2-(((Benzyloxy)carbonyl)amino)-2-hydroxyacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl carbamate | HCID 12136 | — |
| Reactant | Glyoxylic acid, monohydrate | HCID 15620607 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(((Benzyloxy)carbonyl)amino)-2-hydroxyacetic acid | HCID 3509506 | 73% |
Reaction Steps
Benzyl carbamate (63 g, 0.05 mol) was stirred with glyoxylic acid monohydrate (5.09 g, 0.055 mol) in dry ether (50 mL). The crystalline product 22A (7.81 g, 73%) formed was filtered and washed with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776902 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-82e393e4c9094256a6fe424d4b40a20a |
| Source note | uspto-grants-1998_07 |