Phosgene → HCID 19071309, compound

HRID 1955624Notes

Reaction equation

HRID 1955624 reaction equation
[CH:1]1([CH2:6][NH2:7])[CH2:5][CH2:4][CH2:3][CH2:2]1.[C:8](Cl)(Cl)=[O:9]>>[CH:1]1([CH2:6][NH:7][C:8]([NH:7][CH2:6][CH:1]2[CH2:5][CH2:4][CH2:3][CH2:2]2)=[O:9])[CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 6371PhosgeneHCID 80153Cyclopentanemethylamine

Product 1

HCID 19071309HCID 19071309, compoundYield 81%

Procedure

In the manner of step (a) of Example 1, cyclopentanemethylamine (K. Jewers and J. McKenna, J. Chem. Soc. 1958, 2209-2217; 23.0 g, 0.158 mole) was reacted with phosgene to give 1,3-bis(cyclopentylmethyl)urea as white powder (14.41 g, 81%), m.p. 162°-164° C.;

Sources & evidence

ORD record
ord-7e71e44dab894800a1e9217aa2841030
Source dataset
uspto-grants-1998_07
Patent number
US05776940

Reaction notes

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