HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 19071315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 1-Cyclobutylmethanamine hydrochloride | HCID 21707944 | — |
| Product | HCID 19071315 | HCID 19071315 | 37% |
Reaction Steps
In the manner of step (a) of Example 1, cyclobutanemethylamine hydrochloride (Buchman and Howton, J. Amer. Chem. Soc. 1948, 70:2517; 7.96 g, 80.5 mmol) was reacted with phosgene to give 1,3-bis(cyclobutylmethyl)urea as white powder (5.20 g, 37%), m.p. 153°-155° C.; 1H-NMR (DMSO-d6) consistent with structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776940 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-f13cc41b5a7d4244a699c162464343d4 |
| Source note | uspto-grants-1998_07 |