HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 11673521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 2-(1-Cyclohexenyl)ethylamine | HCID 76938 | — |
| Product | HCID 11673521 | HCID 11673521 | 54% |
Reaction Steps
In the manner of step (a) of Example 6, 2-(1-cyclohexenyl)ethylamine (Aldrich, 94.6 g, 0.733 mole as 97%) was reacted with 1,1'-carbonyldiimidazole to give 1,3-bis[2-(1-cyclohexen-1-yl)ethyl]urea as a white powder (56.26 g, 54%), m.p. 129°-131° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776940 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-9d1bf7075e2340378120bf1a9a4a8024 |
| Source note | uspto-grants-1998_07 |