HCID 11673521, compound → HCID 19071310, compound

HRID 1955631Notes

Reaction equation

HRID 1955631 reaction equation
[C:1]1([CH2:7][CH2:8][NH:9][C:10]([NH:12][CH2:13][CH2:14][C:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH:16]=2)=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.C1(CCN2[C:34](=[O:35])[CH:33]=[CH:32][NH:31]C2=O)CCCCC=1>>[NH2:31][C:32]1[N:9]([CH2:8][CH2:7][C:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=2)[C:10](=[O:11])[N:12]([CH2:13][CH2:14][C:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH:16]=2)[C:34](=[O:35])[CH:33]=1

Participants

3

Reactant 2

HCID 11673521HCID 11673521, compoundHCID 67659265HCID 67659265, compound

Product 1

HCID 19071310HCID 19071310, compoundYield 85%

Procedure

In the manner of step (b) of Example 1, 1,3-bis[2-(1-cyclohexen-1-yl)ethyl]urea (from step (a), 55.00 g, 0.199 mol) was converted to 6-amino-1,3-bis[(2-(cyclohexen-1-yl)ethyl]uracil, isolated as a white powder (58.03 g, 85%), m.p. 172°-174° C.;

Sources & evidence

ORD record
ord-ee430dde105347dca47cc7b4a34ebb14
Source dataset
uspto-grants-1998_07
Patent number
US05776940

Reaction notes

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