HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 70142577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 70143857 | HCID 70143857 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 70142577 | HCID 70142577 | 130.8% |
Reaction Steps
Ethyl N-chloroacetyl-4-aminomethylsalicylate (0.11 g, 0.40 mmoles) was dissolved in acetone (5 mL) and sodium iodide (0.06 g, 0.40 mmoles) was added. The solution was refluxed for 2.5 hours, then cooled to room temperature and filtered. The filtrate was evaporated to dryness to afford a white solid of ethyl N-iodoacetyl-4-aminomethylsalicylate (0.19 g, 100% yield) (m.p. 105°-108° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05777148 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-80962ac25f154a78bdd4ea5f56db2413 |
| Source note | uspto-grants-1998_07 |