Thionyl Chloride → HCID 14794243, compound

HRID 1956089Notes

Reaction equation

HRID 1956089 reaction equation
[CH2:1]([CH:6]1[CH2:11][CH2:10][CH:9]([CH:12]2[CH2:17][CH2:16][CH:15]([CH2:18][C:19]([OH:21])=O)[CH2:14][CH2:13]2)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5].S(Cl)([Cl:24])=O>>[CH2:1]([CH:6]1[CH2:11][CH2:10][CH:9]([CH:12]2[CH2:17][CH2:16][CH:15]([CH2:18][C:19]([Cl:24])=[O:21])[CH2:14][CH2:13]2)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 18604893HCID 18604893, compound

Product 1

HCID 14794243HCID 14794243, compound

Procedure

A mixture of 50 g (0.17 mol) of 4-(4-pentylcyclohexyl) cyclohexyl acetic acid and 135 Ml of thionyl chloride was heated for 4 hours to reflux. Excess amount of thionyl chloride was separated under a reduced pressure to obtain 4-(4-pentylcyclohexyl)cyclohexyl acetic acid chloride.

Workup

  1. temperaturewas heated for 4 hours
  2. temperatureto reflux
  3. customExcess amount of thionyl chloride was separated under a reduced pressure

Sources & evidence

ORD record
ord-040ff91dcbeb4c2e9364b665430e5615
Source dataset
uspto-grants-1998_07
Patent number
US05779936

Reaction notes

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