反应详情

A mixture of 50 g (0.17 mol) of 4-(4-pentylcyclohexyl) cyclohexyl acetic acid and 135 Ml of thionyl chloride was heated for 4 hours to reflux. Excess amount of thionyl chloride was separated under a reduced pressure to obtain 4-(4-pentylcyclohexyl)cyclohexyl acetic acid chloride.

1. temperaturewas heated for 4 hours
2. temperatureto reflux
3. customExcess amount of thionyl chloride was separated under a reduced pressure