HCID 18663043, compound → HCID 18663092, compound
Reaction equation
C1(O[C:8](=[O:21])[NH:9][C:10]2[C:11]([O:19][CH3:20])=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[C:22]([O:25][C:26]1[CH:27]=[C:28]([N:34]2[CH2:39][CH2:38][NH:37][CH2:36][CH2:35]2)[CH:29]=[CH:30][C:31]=1[O:32][CH3:33])(=[O:24])[CH3:23]>>[CH2:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:37]2[CH2:38][CH2:39][N:34]([C:28]3[CH:29]=[CH:30][C:31]([O:32][CH3:33])=[C:26]([O:25][C:22](=[O:24])[CH3:23])[CH:27]=3)[CH2:35][CH2:36]2)=[O:21])[C:11]([O:19][CH3:20])=[N:12][C:13]=1[CH3:18])[CH3:17]Participants
3
Procedure
Phenyl-N-(5-ethyl-2-methoxy-6-methylpyridin-3-yl)carbamate and 1-(3-acetoxy-4-methoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound. 25 yield: 62% Example 54
Sources & evidence
- ORD record
- ord-acf12f4fcb6e42189c44f64b8d2c6005
- Source dataset
- uspto-grants-1998_07
- Patent number
- US05780472
Reaction notes
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