1-(2-Methoxyphenyl)piperazine → HCID 18663030, compound

HRID 1956249Notes

Reaction equation

HRID 1956249 reaction equation
C1(O[C:8](=[O:22])[NH:9][C:10]2[C:11]([O:19][CH2:20][CH3:21])=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[CH3:23][O:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[N:31]1[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]1>>[CH2:20]([O:19][C:11]1[C:10]([NH:9][C:8]([N:34]2[CH2:33][CH2:32][N:31]([C:26]3[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=3[O:24][CH3:23])[CH2:36][CH2:35]2)=[O:22])=[CH:15][C:14]([CH2:16][CH3:17])=[C:13]([CH3:18])[N:12]=1)[CH3:21]

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 18663163HCID 18663163, compound

Product 1

HCID 18663030HCID 18663030, compoundYield 82%

Procedure

Phenyl-N-(2-ethoxy-5-ethyl-6-methylpyridin-3-yl)carbamate and 1-(2-methoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-208f4b6e43fb43bcafe48ee51d698427
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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