1-(3,5-Dichlorophenyl)piperazine → HCID 18663142, compound

HRID 1956259Notes

Reaction equation

HRID 1956259 reaction equation
C1(O[C:8](=[O:26])[NH:9][C:10]2[C:11]([O:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[Cl:27][C:28]1[CH:29]=[C:30]([N:35]2[CH2:40][CH2:39][NH:38][CH2:37][CH2:36]2)[CH:31]=[C:32]([Cl:34])[CH:33]=1>>[CH2:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:38]2[CH2:37][CH2:36][N:35]([C:30]3[CH:29]=[C:28]([Cl:27])[CH:33]=[C:32]([Cl:34])[CH:31]=3)[CH2:40][CH2:39]2)=[O:26])[C:11]([O:19][C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)=[N:12][C:13]=1[CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 27360671-(3,5-Dichlorophenyl)piperazineHCID 18663175HCID 18663175, compound

Product 1

HCID 18663142HCID 18663142, compoundYield 82%

Procedure

Phenyl-N-(5-ethyl-6-methyl-2-phenoxypyridin-3-yl)carbamate and 1-(3,5-dichlorophenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-da538f25b69d4953b40ab6faa715e88a
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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