1-(2-Methoxyphenyl)piperazine → HCID 18663138, compound

HRID 1956262Notes

Reaction equation

HRID 1956262 reaction equation
C1(O[C:8](=[O:21])[NH:9][C:10]2[C:11]([NH:19][CH3:20])=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[CH3:22][O:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=1[N:30]1[CH2:35][CH2:34][NH:33][CH2:32][CH2:31]1>>[CH2:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:33]2[CH2:32][CH2:31][N:30]([C:25]3[CH:26]=[CH:27][CH:28]=[CH:29][C:24]=3[O:23][CH3:22])[CH2:35][CH2:34]2)=[O:21])[C:11]([NH:19][CH3:20])=[N:12][C:13]=1[CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 19357187HCID 19357187, compound

Product 1

HCID 18663138HCID 18663138, compoundYield 73%

Procedure

Phenyl-N-(5-ethyl-6-methyl-2-methylaminopyridin-3-yl)carbamate and 1-(2-methoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-230a229734be404eb6fe102388a34529
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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