1-(3,5-Dimethoxyphenyl)piperazine → HCID 18663139, compound

HRID 1956263Notes

Reaction equation

HRID 1956263 reaction equation
C1(O[C:8](=[O:21])[NH:9][C:10]2[C:11]([NH:19][CH3:20])=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[CH3:22][O:23][C:24]1[CH:25]=[C:26]([N:32]2[CH2:37][CH2:36][NH:35][CH2:34][CH2:33]2)[CH:27]=[C:28]([O:30][CH3:31])[CH:29]=1>>[CH2:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:35]2[CH2:34][CH2:33][N:32]([C:26]3[CH:25]=[C:24]([O:23][CH3:22])[CH:29]=[C:28]([O:30][CH3:31])[CH:27]=3)[CH2:37][CH2:36]2)=[O:21])[C:11]([NH:19][CH3:20])=[N:12][C:13]=1[CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 27362051-(3,5-Dimethoxyphenyl)piperazineHCID 19357187HCID 19357187, compound

Product 1

HCID 18663139HCID 18663139, compoundYield 82%

Procedure

Phenyl-N-(5-ethyl-6-methyl-2-methylaminopyridin-3-yl)carbamate and 1-(3,5-dimetoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-63ed067be9a54e97b38da626c4e83fde
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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