1-(2-Methoxyphenyl)piperazine → HCID 18663150, compound

HRID 1956264Notes

Reaction equation

HRID 1956264 reaction equation
C1(O[C:8](=[O:19])[NH:9][C:10]2[CH:11]=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[CH3:20][O:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][C:23]=1[N:28]1[CH2:33][CH2:32][NH:31][CH2:30][CH2:29]1>>[CH2:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:31]2[CH2:30][CH2:29][N:28]([C:23]3[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=3[O:21][CH3:20])[CH2:33][CH2:32]2)=[O:19])[CH:11]=[N:12][C:13]=1[CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 18663176HCID 18663176, compound

Product 1

HCID 18663150HCID 18663150, compoundYield 80%

Procedure

Phenyl-N-(5-ethyl-6-methylpyridin-3-yl)carbamate and 1-(2-methoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-750656575a2241ea9d1a2029f443e0cd
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

Loading…