1-(3,5-Dimethoxyphenyl)piperazine → HCID 18663151, compound

HRID 1956265Notes

Reaction equation

HRID 1956265 reaction equation
C1(O[C:8](=[O:19])[NH:9][C:10]2[CH:11]=[N:12][C:13]([CH3:18])=[C:14]([CH2:16][CH3:17])[CH:15]=2)C=CC=CC=1.[CH3:20][O:21][C:22]1[CH:23]=[C:24]([N:30]2[CH2:35][CH2:34][NH:33][CH2:32][CH2:31]2)[CH:25]=[C:26]([O:28][CH3:29])[CH:27]=1>>[CH2:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:33]2[CH2:32][CH2:31][N:30]([C:24]3[CH:23]=[C:22]([O:21][CH3:20])[CH:27]=[C:26]([O:28][CH3:29])[CH:25]=3)[CH2:35][CH2:34]2)=[O:19])[CH:11]=[N:12][C:13]=1[CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 27362051-(3,5-Dimethoxyphenyl)piperazineHCID 18663176HCID 18663176, compound

Product 1

HCID 18663151HCID 18663151, compoundYield 85%

Procedure

Phenyl-N-(5-ethyl-6-methylpyridin-3-yl)carbamate and 1-(3,5-dimethoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-e22c686b13cd4742bd140d1e74fef8e4
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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