1-(2,3-Xylyl)piperazine → HCID 18663052, compound

HRID 1956277Notes

Reaction equation

HRID 1956277 reaction equation
C1(O[C:8](=[O:20])[NH:9][C:10]2[C:11]([O:18][CH3:19])=[N:12][C:13]([CH3:17])=[C:14]([CH3:16])[CH:15]=2)C=CC=CC=1.[C:21]1([N:29]2[CH2:34][CH2:33][NH:32][CH2:31][CH2:30]2)[CH:26]=[CH:25][CH:24]=[C:23]([CH3:27])[C:22]=1[CH3:28]>>[CH3:16][C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:32]2[CH2:33][CH2:34][N:29]([C:21]3[CH:26]=[CH:25][CH:24]=[C:23]([CH3:27])[C:22]=3[CH3:28])[CH2:30][CH2:31]2)=[O:20])[C:11]([O:18][CH3:19])=[N:12][C:13]=1[CH3:17]

Participants

3

Reactant 2

HCID 705411-(2,3-Xylyl)piperazineHCID 11086894Phenyl N-(5,6-dimethyl-2-methoxypyridin-3-yl)carbamate

Product 1

HCID 18663052HCID 18663052, compoundYield 72%

Procedure

Phenyl-N-(5,6-dimethyl-2-methoxypyridin-3-yl)carbamate and 1-(2,3-xylyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-c716dbd890fc43f2811876c97c423ba5
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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