Phenyl N-(5,6-dimethyl-2-methoxypyridin-3-yl)carbamate → HCID 18663054, compound

HRID 1956280Notes

Reaction equation

HRID 1956280 reaction equation
C1(O[C:8](=[O:20])[NH:9][C:10]2[C:11]([O:18][CH3:19])=[N:12][C:13]([CH3:17])=[C:14]([CH3:16])[CH:15]=2)C=CC=CC=1.[OH:21][C:22]1[CH:27]=[C:26]([CH3:28])[CH:25]=[CH:24][C:23]=1[N:29]1[CH2:34][CH2:33][NH:32][CH2:31][CH2:30]1>>[CH3:16][C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:32]2[CH2:31][CH2:30][N:29]([C:23]3[CH:24]=[CH:25][C:26]([CH3:28])=[CH:27][C:22]=3[OH:21])[CH2:34][CH2:33]2)=[O:20])[C:11]([O:18][CH3:19])=[N:12][C:13]=1[CH3:17]

Participants

3

Reactant 2

HCID 11086894Phenyl N-(5,6-dimethyl-2-methoxypyridin-3-yl)carbamateHCID 18663031HCID 18663031, compound

Product 1

HCID 18663054HCID 18663054, compoundYield 77%

Procedure

Phenyl-N-(5,6-dimethyl-2-methoxypyridin-3-yl)carbamate and 1-(2-hydroxy-4-methylphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-511aa1cdec2747999a56533de80c1866
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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