1-(2-Methoxyphenyl)piperazine → HCID 18663153, compound

HRID 1956291Notes

Reaction equation

HRID 1956291 reaction equation
C1(O[C:8](=[O:22])[NH:9][C:10]2[C:11]([O:20][CH3:21])=[N:12][C:13]([CH3:19])=[C:14]([CH:16]([CH3:18])[CH3:17])[CH:15]=2)C=CC=CC=1.[CH3:23][O:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[N:31]1[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]1>>[CH:16]([C:14]1[CH:15]=[C:10]([NH:9][C:8]([N:34]2[CH2:33][CH2:32][N:31]([C:26]3[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=3[O:24][CH3:23])[CH2:36][CH2:35]2)=[O:22])[C:11]([O:20][CH3:21])=[N:12][C:13]=1[CH3:19])([CH3:17])[CH3:18]

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 18663177HCID 18663177, compound

Product 1

HCID 18663153HCID 18663153, compoundYield 64%

Procedure

Phenyl-N-(5-isopropyl-2-methoxy-6-methylpyridin-3-yl)carbamate and 1-(2-methoxyphenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-fadbdf96184f4495aeff371a842183f1
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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