1-(3-Chlorophenyl)piperazine → HCID 18663039, compound

HRID 1956297Notes

Reaction equation

HRID 1956297 reaction equation
C1(O[C:8](=[O:18])[NH:9][C:10]2[C:11]([O:16][CH3:17])=[N:12][CH:13]=[CH:14][CH:15]=2)C=CC=CC=1.[Cl:19][C:20]1[CH:21]=[C:22]([N:26]2[CH2:31][CH2:30][NH:29][CH2:28][CH2:27]2)[CH:23]=[CH:24][CH:25]=1>>[CH3:17][O:16][C:11]1[C:10]([NH:9][C:8]([N:29]2[CH2:28][CH2:27][N:26]([C:22]3[CH:23]=[CH:24][CH:25]=[C:20]([Cl:19])[CH:21]=3)[CH2:31][CH2:30]2)=[O:18])=[CH:15][CH:14]=[CH:13][N:12]=1

Participants

3

Reactant 2

HCID 13551-(3-Chlorophenyl)piperazineHCID 18663166HCID 18663166, compound

Product 1

HCID 18663039HCID 18663039, compoundYield 72%

Procedure

Phenyl-N-(2-methoxypyridin-3-yl)carbamate and 1-(3-chlorophenyl)piperazine were reacted by the same way with the example 1 to obtain the titled compound.

Sources & evidence

ORD record
ord-092c7ac516164fdf93dd25e676207551
Source dataset
uspto-grants-1998_07
Patent number
US05780472

Reaction notes

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