HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → 4-(Phenylthio)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 4-Bromobenzoic acid | HCID 11464 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Product | 4-(Phenylthio)benzoic acid | HCID 238598 | 95.7% |
Reaction Steps
The conditions to prepare Reference Example 32 cl384847 are used with 6.0 g of mercaptobenzene, 12.22 g of potassium t-butoxide and 13.15 g of 4-bromobenzoic acid to give 12.0 g of the desired product as a solid, m.p. 101°-103° C.; M+H=231.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780471 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-e62fd59dacd9478395f3d95f83dd7208 |
| Source note | uspto-grants-1998_07 |