Thionyl Chloride → 4-Benzoylbenzoyl chloride

HRID 1956322Notes

Reaction equation

HRID 1956322 reaction equation
[C:1]([C:9]1[CH:17]=[CH:16][C:12]([C:13](O)=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.S(Cl)([Cl:20])=O>C(Cl)Cl>[C:1]([C:9]1[CH:17]=[CH:16][C:12]([C:13]([Cl:20])=[O:14])=[CH:11][CH:10]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 691474-Benzoylbenzoic acid

Product 1

HCID 129121414-Benzoylbenzoyl chloride

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The conditions to prepare Reference Example 34 are used with 2.0 g of 4-benzoylbenzoic acid and 30 ml of thionyl chloride to give the desired product in a solution of 30 ml of methylene chloride.

Workup

  1. customThe conditions to prepare Reference Example 34

Sources & evidence

ORD record
ord-ae878323e1a14ef59c486a8cfa3caef4
Source dataset
uspto-grants-1998_07
Patent number
US05780471

Reaction notes

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