HRID1956410

反应详情

EQUATION

反应方程式

HRID 1956410 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Ethyl-5-nitropyridine (16.3 g) was dissolved in IMS (200 ml) and hydrogenated at ambient temperature at 1 atmosphere using 10% palladium charcoal (0.5 g) as the catalyst. The mixture was filtered to remove the catalyst and the filtrate evaporated to give 5-amino-2-ethylpyridine as an oil.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. customto remove the catalyst
  3. customthe filtrate evaporated