HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Phenoxy-3-pyridinamine → HCID 23209227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Phenoxy-3-pyridinamine | HCID 212856 | — |
| Reactant | Ethyl 4-chloro-6-ethoxy-7-methyl-1,8-naphthyridine-3-carboxylate | HCID 23198600 | — |
| Product | HCID 23209227 | HCID 23209227 | — |
Reaction Steps
A mixture of ethyl 4-chloro-6-ethoxy-7-methyl-1,8-naphthyridine-3-carboxylate (2.3 g), 5-amino-2-phenoxypyridine (1.52 g) and IMS (50 ml) was boiled under reflux for 2 hours. The mixture was cooled in ice and filtered to give ethyl 6-ethoxy-7-methyl-4-(2-phenoxy-5-pyridylamino)-1,8-naphthyridine-3-carboxylate hydrochloride, m.p. 220°-221° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780482 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-d346ba19229d4c078220a615686e1dbd |
| Source note | uspto-grants-1998_07 |