HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrothiophene → HCID 21249890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrothiophene | HCID 1127 | — |
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Product | HCID 21249890 | HCID 21249890 | — |
Reaction Steps
To a solution of prenyl bromide (2.9 g in 10 mL dry tetrahydrofuran) at 0° C. was added 1.8 mL tetrahydrothiophene and the mixture allowed to warm to room temperature. After 22 hours, the mixture was concentrated in vacuo and the remaining starting materials removed by azeotrope with toluene to give the crude title compound as a white solid (2.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780437 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-64c67c2252a84786996ced87969a46fa |
| Source note | uspto-grants-1998_07 |